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Heat capacities of nanostructured wurtzite and rock salt ZnO: challenges of ZnO nano-phase diagram

Low-temperature heat capacities (Cp) of nanostructured rock salt (rs-ZnO) and wurtzite (w-ZnO) polymorphs of zinc oxide were measured in the 2-315 K temperature range. No significant influence of nanostructuring on Cp of w-ZnO has been observed. The measured Cp of rock salt ZnO is lower than that of wurtzite ZnO below 100 K and is higher above this temperature. Using available thermodynamic data, we established that the equilibrium pressure between nanocrystalline w-ZnO and rs-ZnO is close to 4.6 GPa at 300 K (half as much as the onset pressure of direct phase transformation) and slightly changes with temperature up to 1000 K.

preprint2021arXivOpen access
Konstantin V. KamenevAlexandre CouracPetr S. SokolovAndrei N. BaranovFelix Yu. SharikovVladimir L. Solozhenko
cond-mat.mtrl-sci
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Konstantin V. KamenevAlexandre CouracPetr S. SokolovAndrei N. BaranovFelix Yu. SharikovVladimir L. Solozhenko

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