Abstract
Neutron diffraction has been used to study the lattice and magnetic structures of the insulating and superconducting RbFeSe. For the insulating RbFeSe, neutron polarization analysis and single crystal neutron diffraction unambiguously confirm the earlier proposed block antiferromagnetic structure. For superconducting samples ( K), we find that in addition to the tetragonal superlattice structure transition at 513 K, the material develops a separate superlattice structure at a lower temperature of 480 K. These results suggest that superconducting RbFeSe is phase separated with coexisting and superlattice structures.
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