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Structural Distortion and Disappearance of Layer Ordering in LixCoO2x2H2O

The structure of a new member of the AxCoO2 x nH2O family (A=Li,Na,K) was determined by high-resolution synchrotron X-ray powder diffraction. Layered lithium cobalt oxide hydrate LixCoO2 x 2H2O crystallizes in a disordered monoclinic structure (space group C2/m) with lattice parameters a = 4.8915(2) A, b = 2.8239(1) A, c = 10.7033(9) A, beta = 112.386(4)deg. Unlike the superconducting sodium cobalt oxide hydrate, this material possesses a structure with lithium-water layers intercalated between disordered octahedral sheets of cobalt oxide. The interlayer spacing is slightly larger (~0.9%) due to the higher water content, and one of the two lithium sites extends into the water layer. This material shows no superconducting transition above 2K.

preprint2004arXivOpen access
Sangmoon ParkYongjae LeeThomas Vogt
cond-mat.supr-concond-mat.mtrl-sci
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Sangmoon ParkYongjae LeeThomas Vogt

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