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Paper detail

Ca_25Co_22O_56(OH)_28: a layered misfit compound

The high pressure synthesis, structure and magnetic properties of Ca_25Co_22O_56(OH)_28 are reported. The compound has a misfit structure, consisting of double, square calcium oxide hydroxide rock-salt-like layers between hexagonal CoO_2 layers. The misfit compound crystallizes in the monoclinic space group C2/m, and can be characterized by the coexistence of two subsystems with common a=4.893(5)A, c=8.825(9)A and b=95.745(8) parameters, and different b parameters: b_RS=4.894(5)A, and b_HEX=2.809(3)A, for the rock-salt and hexagonal type planes respectively. The compound shows Curie-Weiss paramagnetism with an antiferromagnetic Weiss temperature of -43K and a reduced Co moment. Substantial deviations from Curie-Weiss behavior are seen below 50K with no indication of magnetic ordering. No superconductivity was observed down to a temperature of 2K.

preprint2005arXivOpen access
T. KlimczukH. W. ZandbergenN. M. van der PersL. ViciuV. L. MillerM. -H. LeeR. J. Cava
cond-mat.mtrl-sci
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T. KlimczukH. W. ZandbergenN. M. van der PersL. ViciuV. L. MillerM. -H. LeeR. J. Cava

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